zldmЗаводская лаборатория. Диагностика материаловIndustrial laboratory. Diagnostics of materials1028-68612588-0187ООО «Издательство «ТЕСТ-ЗЛ»10.26896/1028-6861-2022-88-1-I-49-61zldm-1561Research ArticleИССЛЕДОВАНИЕ СТРУКТУРЫ И СВОЙСТВ. ФИЗИЧЕСКИЕ МЕТОДЫ ИССЛЕДОВАНИЯ И КОНТРОЛЯSTRUCTURE AND PROPERTIES RESEARCH. PHYSICAL METHODS OF RESEARCH AND MONITORINGИсследование in situ процессов горения гетерогенных сред методом динамической рентгенографииIn situ study of heterogeneous media combustion processes by time Resolved XRDКовалевД. Ю.KovalevD. Yu.

Дмитрий Юрьевич Ковалев

142432, Московская обл., г. Черноголовка, ул. Академика Осипьяна, д. 8

Dmitry Yu. Kovalev

8, ul. Akademika Osipyana, Chernogolovka, Moscow obl., 142432

kovalev@ism.ac.ruПономаревВ. И.PonomarevV. I.

Василий Иванович Пономарев

142432, Московская обл., г. Черноголовка, ул. Академика Осипьяна, д. 8

Vasily I. Ponomarev

8, ul. Akademika Osipyana, Chernogolovka, Moscow obl., 142432

АлымовМ. И.AlymovM. I.

Михаил Иванович Алымов

142432, Московская обл., г. Черноголовка, ул. Академика Осипьяна, д. 8

Mikhail I. Alymov

8, ul. Akademika Osipyana, Chernogolovka, Moscow obl., 142432

Институт структурной макрокинетики проблем материаловедения имени А. Г. Мержанова РАНРоссияA. G. Merzhanov Institute of Structural Macrokinetics and Materials Science, Russian Academy of SciencesRussian Federation202218012022881(I)4961Copyright © Ковалев Д.Ю., Пономарев В.И., Алымов М.И., 20222022Ковалев Д.Ю., Пономарев В.И., Алымов М.И.Kovalev D.Y., Ponomarev V.I., Alymov M.I.Данная работа распространяется под лицензией Creative Commons Attribution 4.0.This work is licensed under a Creative Commons Attribution 4.0 License.https://www.zldm.ru/jour/article/view/1561

При исследованиях конденсированных веществ в процессе химических реакций и фазовых превращений необходимы in situ методы диагностики, позволяющие получать данные о структуре и составе материала в режиме реального времени. В работе представлены результаты диагностики быстропротекающих процессов в гетерогенных конденсированных средах, в том числе самораспространяющегося высокотемпературного синтеза, методом динамической рентгенографии. Метод основан на применении скоростной регистрации дифракционных спектров в широком угловом интервале и дает возможность получать in situ информацию об эволюции кристаллической структуры реагирующих веществ. В качестве источника излучения использовали рентгеновскую трубку. На базе порошкового дифрактометра, быстродействующего линейного детектора и реакционных камер разработана эффективная система анализа с разрешением по времени в диапазоне 10–1 – 102 с. Создан комплекс объектно-ориентированных дифракционных методик для исследования динамики фазовых переходов при самораспространяющемся высокотемпературном синтезе неорганических материалов, горении энергетических систем и жидких растворов, кристаллизации аморфных сплавов, при анализе фазового состава материалов в процессе термической обработки. Полученные результаты могут быть использованы для выявления механизма структурно-химических превращений в конденсированных средах.

The use of in situ diagnostic methods is required to obtain data on the structure and composition of the material in real time when studying condensed substances in the course of chemical reactions and phase transformations. We present the results on the development and application of the time-resolved X-ray diffraction method for the diagnosis of fast processes in heterogeneous condensed media, including self-propagating high-temperature synthesis. An X-ray tube was used as a radiation source. The method is based on the use of high-speed registration of XRD patterns in a wide angular interval and provides obtaining in situ data on the evolution of the crystal structure of the reactants. A high-speed linear detector and reaction chambers, an effective analysis system with a time resolution in the range of 10–1 – 102 sec has been developed on the base of a powder diffractometer. A complex of object-oriented diffraction techniques has been developed to study the dynamics of phase transitions in self-propagating high-temperature synthesis of inorganic materials, combustion of energy systems and liquid solutions, crystallization of amorphous alloys, in the analysis of the phase composition of materials in the process of heat treatment. The results obtained can be used to identify the mechanism of structural and chemical transformations in condensed matter.

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