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<article article-type="research-article" dtd-version="1.3" xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance" xml:lang="ru"><front><journal-meta><journal-id journal-id-type="publisher-id">zldm</journal-id><journal-title-group><journal-title xml:lang="ru">Заводская лаборатория. Диагностика материалов</journal-title><trans-title-group xml:lang="en"><trans-title>Industrial laboratory. Diagnostics of materials</trans-title></trans-title-group></journal-title-group><issn pub-type="ppub">1028-6861</issn><issn pub-type="epub">2588-0187</issn><publisher><publisher-name>ООО «Издательство «ТЕСТ-ЗЛ»</publisher-name></publisher></journal-meta><article-meta><article-id pub-id-type="doi">10.26896/1028-6861-2022-88-12-51-63</article-id><article-id custom-type="elpub" pub-id-type="custom">zldm-1818</article-id><article-categories><subj-group subj-group-type="heading"><subject>Research Article</subject></subj-group><subj-group subj-group-type="section-heading" xml:lang="ru"><subject>ИССЛЕДОВАНИЕ СТРУКТУРЫ И СВОЙСТВ. МЕХАНИКА МАТЕРИАЛОВ: ПРОЧНОСТЬ, РЕСУРС, БЕЗОПАСНОСТЬ</subject></subj-group><subj-group subj-group-type="section-heading" xml:lang="en"><subject>TESTING OF STRUCTURE AND PARAMETERS. MECHANICAL TESTING METHODS</subject></subj-group></article-categories><title-group><article-title>Методы определения характеристик адгезии в системах с теплозащитными покрытиями</article-title><trans-title-group xml:lang="en"><trans-title>Methods for characterizing the interfacial adhesion in thermal barrier coating systems</trans-title></trans-title-group></title-group><contrib-group><contrib contrib-type="author" corresp="yes"><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Федорова</surname><given-names>Е. Н.</given-names></name><name name-style="western" xml:lang="en"><surname>Fedorova</surname><given-names>E. N.</given-names></name></name-alternatives><bio xml:lang="ru"><p>Федорова Елена Николаевна.</p><p>660041, Красноярск, Свободный просп., д. 79; 660049, Красноярск, просп. Мира, д. 53</p></bio><bio xml:lang="en"><p>Elena N. Fedorova.</p><p>79, Svobodny prosp., Krasnoyarsk, 660041; 53, prosp. Mira, Krasnoyarsk, 660049</p></bio><xref ref-type="aff" rid="aff-1"/></contrib><contrib contrib-type="author" corresp="yes"><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Суходоева</surname><given-names>Н. В.</given-names></name><name name-style="western" xml:lang="en"><surname>Sukhodoeva</surname><given-names>N. V.</given-names></name></name-alternatives><bio xml:lang="ru"><p>Суходоева Надежда Вячеславовна.</p><p>660041, Красноярск, Свободный просп., д. 79</p></bio><bio xml:lang="en"><p>Nadezhda V. Sukhodoeva.</p><p>79, Svobodny prosp., Krasnoyarsk, 660041</p></bio><email xlink:type="simple">suhodoevanadezda@gmail.com</email><xref ref-type="aff" rid="aff-2"/></contrib><contrib contrib-type="author" corresp="yes"><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Москвичев</surname><given-names>В. В.</given-names></name><name name-style="western" xml:lang="en"><surname>Moskvichev</surname><given-names>V. V.</given-names></name></name-alternatives><bio xml:lang="ru"><p>Москвичев Владимир Викторович.</p><p>660041, Красноярск, Свободный просп., д. 79; 660049, Красноярск, просп. Мира, д. 53</p></bio><bio xml:lang="en"><p>Vladimir V. Moskvichev.</p><p>79, Svobodny prosp., Krasnoyarsk, 660041; 53, prosp. Mira, Krasnoyarsk, 660049</p></bio><xref ref-type="aff" rid="aff-1"/></contrib><contrib contrib-type="author" corresp="yes"><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Огорельцева</surname><given-names>Н. В.</given-names></name><name name-style="western" xml:lang="en"><surname>Ogoreltceva</surname><given-names>N. V.</given-names></name></name-alternatives><bio xml:lang="ru"><p>Огорельцева Нина Валерьевна.</p><p>660041, Красноярск, Свободный просп., д. 79</p></bio><bio xml:lang="en"><p>Nina V. Ogoreltceva.</p><p>79, Svobodny prosp., Krasnoyarsk, 660041</p></bio><xref ref-type="aff" rid="aff-2"/></contrib><contrib contrib-type="author" corresp="yes"><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Климкин</surname><given-names>Ю. О.</given-names></name><name name-style="western" xml:lang="en"><surname>Klimkin</surname><given-names>Yu. O.</given-names></name></name-alternatives><bio xml:lang="ru"><p>Климкин Юрий Олегович.</p><p>660041, Красноярск, Свободный просп., д. 79</p></bio><bio xml:lang="en"><p>Yuri O. Klimkin.</p><p>79, Svobodny prosp., Krasnoyarsk, 660041</p></bio><xref ref-type="aff" rid="aff-2"/></contrib></contrib-group><aff-alternatives id="aff-1"><aff xml:lang="ru"><institution>Сибирский федеральный университет; Красноярский филиал Федерального исследовательского центра информационных и вычислительных технологий</institution><country>Россия</country></aff><aff xml:lang="en"><institution>Siberian Federal University; Krasnoyarsk Branch of the Federal Research Center for Information and Computational Technologies</institution><country>Russian Federation</country></aff></aff-alternatives><aff-alternatives id="aff-2"><aff xml:lang="ru"><institution>Сибирский федеральный университет</institution><country>Россия</country></aff><aff xml:lang="en"><institution>Siberian Federal University</institution><country>Russian Federation</country></aff></aff-alternatives><pub-date pub-type="collection"><year>2022</year></pub-date><pub-date pub-type="epub"><day>25</day><month>12</month><year>2022</year></pub-date><volume>88</volume><issue>12</issue><fpage>51</fpage><lpage>63</lpage><permissions><copyright-statement>Copyright &amp;#x00A9; Федорова Е.Н., Суходоева Н.В., Москвичев В.В., Огорельцева Н.В., Климкин Ю.О., 2022</copyright-statement><copyright-year>2022</copyright-year><copyright-holder xml:lang="ru">Федорова Е.Н., Суходоева Н.В., Москвичев В.В., Огорельцева Н.В., Климкин Ю.О.</copyright-holder><copyright-holder xml:lang="en">Fedorova E.N., Sukhodoeva N.V., Moskvichev V.V., Ogoreltceva N.V., Klimkin Y.O.</copyright-holder><license xml:lang="ru" license-type="creative-commons-attribution" xlink:href="https://creativecommons.org/licenses/by/4.0/" xlink:type="simple"><license-p>Данная работа распространяется под лицензией Creative Commons Attribution 4.0.</license-p></license><license xml:lang="en" license-type="creative-commons-attribution" xlink:href="https://creativecommons.org/licenses/by/4.0/" xlink:type="simple"><license-p>This work is licensed under a Creative Commons Attribution 4.0 License.</license-p></license></permissions><self-uri xlink:href="https://www.zldm.ru/jour/article/view/1818">https://www.zldm.ru/jour/article/view/1818</self-uri><abstract><p>Системы теплозащитных покрытий (ТЗП) широко используют в современных высокотемпературных авиационных газовых турбинах для защиты поверхностей лопаток от газовой коррозии и воздействия высоких рабочих температур. Для прогнозирования долговечности систем с ТЗП одним из ключевых является параметр, характеризующий сопротивление отслоению (адгезию) на поверхностях раздела. Цель работы — анализ существующих методов количественного определения характеристик адгезии для многослойных теплозащитных покрытий и защитных оксидных слоев на поверхности жаропрочных сплавов на основе никеля и выявление причин разброса показателей адгезии. Рассмотрены теоретические предпосылки для определения характеристик адгезии. Показано отсутствие национальных стандартов для их оценки и отмечен значительный разброс значений, полученных при использовании международных документов, регламентирующих испытания, и авторских методик. Значения интенсивности высвобождения упругой энергии деформации варьируются 0,3 до 230 Дж/м2 в зависимости от метода определения, условий эксперимента и параметров системы. Причины разброса значений условно разделены на две группы: 1 — внутренние, обусловленные особенностями формирования слоев ТЗП и температурным воздействием, определяющие величину и характер распределения остаточных деформаций и напряжений, а также направление, по которому инициируется разрушение; 2 — внешние, обусловленные особенностями проведения испытаний и обработки результатов. Показана необходимость комплексного подхода к оценке характеристик адгезии, учитывающего влияние внешних и внутренних факторов.</p></abstract><trans-abstract xml:lang="en"><p>Thermal barrier coatings (TBC) are widely used to protect the hot section structural components, such as aircraft gas turbine, against hot corrosion and large thermal gradients during the service life. The resistance to interfacial debonding (adhesion) is one of the key factors for predicting the TBC durability during operation. The goal of the study is analysis of the existing approaches to quantification of the interfacial adhesion for multi-layered thermal barrier coating systems and thermally-grown oxide on Ni-based superalloys and discussion of the problem regarding the reasons for a large spread of the adhesion characteristics. Theoretical prerequisites for determining the adhesion characteristics are considered to provide a theoretical background for quantification of the interfacial adhesion. The absence of national standard tests applicable to TBC is marked along with a significant scatter of the values obtained using international test-regulating documents and proprietary technologies. The values of the intensity of the strain energy release are found to vary from 0.3 to 230 J/m2 depending on the method for measuring adhesion, experimental details and type of the system considered. The factors that determine a large spread of the interfacial adhesion values were divided into two groups: 1 — intrinsic, attributed to the features of TBC layer formation and temperature affecting the value and distribution of residual strains and stresses and direction of the failure initiation; 2 — extrinsic, which are related to test conditions and technique of experimental data processing. A complex approach involving both intrinsic and extrinsic parameters is required to address the problem of interfacial adhesion quantification.</p></trans-abstract><kwd-group xml:lang="ru"><kwd>система теплозащитных покрытий</kwd><kwd>защитные оксидные слои</kwd><kwd>жаропрочные сплавы на основе никеля</kwd><kwd>поверхности раздела</kwd><kwd>адгезия</kwd><kwd>методы определения характеристик адгезии</kwd></kwd-group><kwd-group xml:lang="en"><kwd>TBC system</kwd><kwd>thermally-grown oxide</kwd><kwd>Ni-based superalloy</kwd><kwd>interfaces</kwd><kwd>adhesion</kwd><kwd>methods for quantification of adhesion characteristics</kwd></kwd-group><funding-group><funding-statement xml:lang="ru">Работа выполнена в рамках государственного задания Министерства науки и высшего образования Российской Федерации (код научной темы FSRZ-2020-0011).</funding-statement></funding-group></article-meta></front><back><ref-list><title>References</title><ref id="cit1"><label>1</label><citation-alternatives><mixed-citation xml:lang="ru">Evans Н. 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