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<article article-type="research-article" dtd-version="1.3" xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance" xml:lang="ru"><front><journal-meta><journal-id journal-id-type="publisher-id">zldm</journal-id><journal-title-group><journal-title xml:lang="ru">Заводская лаборатория. Диагностика материалов</journal-title><trans-title-group xml:lang="en"><trans-title>Industrial laboratory. Diagnostics of materials</trans-title></trans-title-group></journal-title-group><issn pub-type="ppub">1028-6861</issn><issn pub-type="epub">2588-0187</issn><publisher><publisher-name>ООО «Издательство «ТЕСТ-ЗЛ»</publisher-name></publisher></journal-meta><article-meta><article-id pub-id-type="doi">10.26896/1028-6861-2023-89-11-52-59</article-id><article-id custom-type="elpub" pub-id-type="custom">zldm-2060</article-id><article-categories><subj-group subj-group-type="heading"><subject>Research Article</subject></subj-group><subj-group subj-group-type="section-heading" xml:lang="ru"><subject>ИССЛЕДОВАНИЕ СТРУКТУРЫ И СВОЙСТВ</subject></subj-group><subj-group subj-group-type="section-heading" xml:lang="en"><subject>STRUCTURE AND PROPERTIES INVESTIGATION</subject></subj-group></article-categories><title-group><article-title>Исследование электрофизических и магнитных свойств дираковского 3D полуметалла Cd3As2 с наногранулами MnAs</article-title><trans-title-group xml:lang="en"><trans-title>Study of the electrophysical and magnetic properties of a Dirac 3D semimetal Cd3As2 with nanogranules of MnAs</trans-title></trans-title-group></title-group><contrib-group><contrib contrib-type="author" corresp="yes"><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Сайпулаева</surname><given-names>Л. А.</given-names></name><name name-style="western" xml:lang="en"><surname>Saypulaeva</surname><given-names>L. A.</given-names></name></name-alternatives><bio xml:lang="ru"><p>Луиза Абдурахмановна Сайпулаева</p><p>367015, г. Махачкала, ул. М. Ярагского, д. 94</p></bio><bio xml:lang="en"><p>Luiza A. Saypulaeva</p><p>94, ul. M. Yaragskogo, Makhachkala</p></bio><email xlink:type="simple">l.sayplaeva@gmail.com</email><xref ref-type="aff" rid="aff-1"/></contrib><contrib contrib-type="author" corresp="yes"><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Мельникова</surname><given-names>Н. В.</given-names></name><name name-style="western" xml:lang="en"><surname>Melnikova</surname><given-names>N. V.</given-names></name></name-alternatives><bio xml:lang="ru"><p>Нина Владимировна Мельникова</p><p>620002, г. Екатеринбург, ул. Куйбышева, д. 48</p></bio><bio xml:lang="en"><p>Nina V. Melnikova</p><p>48, ul. Kuibysheva, Yekaterinburg, 620002</p></bio><xref ref-type="aff" rid="aff-2"/></contrib><contrib contrib-type="author" corresp="yes"><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Гаджиалиев</surname><given-names>М. М.</given-names></name><name name-style="western" xml:lang="en"><surname>Gadzhialiev</surname><given-names>M. M.</given-names></name></name-alternatives><bio xml:lang="ru"><p>Магомед Магомедович Гаджиалиев</p><p>367015, г. Махачкала, ул. М. Ярагского, д. 94</p></bio><bio xml:lang="en"><p>Magomed M. Gadzhialiev</p><p>94, ul. M. Yaragskogo, Makhachkala, 367015</p></bio><xref ref-type="aff" rid="aff-1"/></contrib><contrib contrib-type="author" corresp="yes"><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Тебеньков</surname><given-names>А. В.</given-names></name><name name-style="western" xml:lang="en"><surname>Tebenkov</surname><given-names>A. V.</given-names></name></name-alternatives><bio xml:lang="ru"><p>Александр Владимирович Тебеньков</p><p>620002, г. Екатеринбург, ул. Куйбышева, д. 48</p></bio><bio xml:lang="en"><p>Alexander V. Tebenkov</p><p>48, ul. Kuibysheva, Yekaterinburg, 620002</p></bio><xref ref-type="aff" rid="aff-2"/></contrib><contrib contrib-type="author" corresp="yes"><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Бабушкин</surname><given-names>А. Н.</given-names></name><name name-style="western" xml:lang="en"><surname>Babushkin</surname><given-names>A. N.</given-names></name></name-alternatives><bio xml:lang="ru"><p>Алексей Николаевич Бабушкин</p><p>620002, г. Екатеринбург, ул. Куйбышева, д. 48</p></bio><bio xml:lang="en"><p>Aleksey N. Babushkin</p><p>48, ul. Kuibysheva, Yekaterinburg, 620002</p><p> </p></bio><xref ref-type="aff" rid="aff-2"/></contrib><contrib contrib-type="author" corresp="yes"><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Захвалинский</surname><given-names>В. С.</given-names></name><name name-style="western" xml:lang="en"><surname>Zakhvalinskii</surname><given-names>V. S.</given-names></name></name-alternatives><bio xml:lang="ru"><p>Василий Сергеевич Захвалинский</p><p>308015, г. Белгород, ул. Победы, д. 85</p><p> </p></bio><bio xml:lang="en"><p>Vasiliy S. Zakhvalinskii</p><p>4, Leninsky prosp., Moscow, 119991</p></bio><xref ref-type="aff" rid="aff-3"/></contrib><contrib contrib-type="author" corresp="yes"><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Аль-Онаизан</surname><given-names>М. Х. А.</given-names></name><name name-style="western" xml:lang="en"><surname>Al-Onaizan</surname><given-names>M. H.</given-names></name></name-alternatives><bio xml:lang="ru"><p>Мохаммад Хассан Али Аль-Онаизан</p><p>Россия, 119991, Москва, Ленинский пр., д. 4</p></bio><bio xml:lang="en"><p>Mohammad H. Al-Onaizan</p><p>4, Leninsky prosp., Moscow, 119991</p></bio><xref ref-type="aff" rid="aff-4"/></contrib><contrib contrib-type="author" corresp="yes"><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Риль</surname><given-names>А. И.</given-names></name><name name-style="western" xml:lang="en"><surname>Ril</surname><given-names>A. I.</given-names></name></name-alternatives><bio xml:lang="ru"><p>Алексей Игоревич Риль</p><p>119991, Москва, Ленинский пр., д. 31</p></bio><bio xml:lang="en"><p>Aleksey I. Ril</p><p>31, Leninsky prosp., Moscow, 119991</p></bio><xref ref-type="aff" rid="aff-5"/></contrib></contrib-group><aff-alternatives id="aff-1"><aff xml:lang="ru"><institution>Институт физики ДФИЦ РАН</institution><country>Россия</country></aff><aff xml:lang="en"><institution>Institute of Physics, DFRC RAS</institution><country>Russian Federation</country></aff></aff-alternatives><aff-alternatives id="aff-2"><aff xml:lang="ru"><institution>Уральский федеральный университет, Институт естественных наук и математики</institution><country>Россия</country></aff><aff xml:lang="en"><institution>Ural Federal University, Institute of Natural Sciences and Mathematics</institution><country>Russian Federation</country></aff></aff-alternatives><aff-alternatives id="aff-3"><aff xml:lang="ru"><institution>Белгородский государственный национальный исследовательский университет</institution><country>Россия</country></aff><aff xml:lang="en"><institution>National University of Science and Technology «MISIS»</institution><country>Russian Federation</country></aff></aff-alternatives><aff-alternatives id="aff-4"><aff xml:lang="ru"><institution>НИТУ «МИСИС»</institution><country>Россия</country></aff><aff xml:lang="en"><institution>National University of Science and Technology «MISIS»</institution><country>Russian Federation</country></aff></aff-alternatives><aff-alternatives id="aff-5"><aff xml:lang="ru"><institution>Институт общей и неорганической химии имени Н. С. Курнакова РАН</institution><country>Россия</country></aff><aff xml:lang="en"><institution>Institute of General and Inorganic Chemistry, RAS</institution><country>Russian Federation</country></aff></aff-alternatives><pub-date pub-type="collection"><year>2023</year></pub-date><pub-date pub-type="epub"><day>21</day><month>11</month><year>2023</year></pub-date><volume>89</volume><issue>11</issue><fpage>52</fpage><lpage>59</lpage><permissions><copyright-statement>Copyright &amp;#x00A9; Сайпулаева Л.А., Мельникова Н.В., Гаджиалиев М.М., Тебеньков А.В., Бабушкин А.Н., Захвалинский В.С., Аль-Онаизан М., Риль А.И., 2023</copyright-statement><copyright-year>2023</copyright-year><copyright-holder xml:lang="ru">Сайпулаева Л.А., Мельникова Н.В., Гаджиалиев М.М., Тебеньков А.В., Бабушкин А.Н., Захвалинский В.С., Аль-Онаизан М., Риль А.И.</copyright-holder><copyright-holder xml:lang="en">Saypulaeva L.A., Melnikova N.V., Gadzhialiev M.M., Tebenkov A.V., Babushkin A.N., Zakhvalinskii V.S., Al-Onaizan M., Ril A.I.</copyright-holder><license xml:lang="ru" license-type="creative-commons-attribution" xlink:href="https://creativecommons.org/licenses/by/4.0/" xlink:type="simple"><license-p>Данная работа распространяется под лицензией Creative Commons Attribution 4.0.</license-p></license><license xml:lang="en" license-type="creative-commons-attribution" xlink:href="https://creativecommons.org/licenses/by/4.0/" xlink:type="simple"><license-p>This work is licensed under a Creative Commons Attribution 4.0 License.</license-p></license></permissions><self-uri xlink:href="https://www.zldm.ru/jour/article/view/2060">https://www.zldm.ru/jour/article/view/2060</self-uri><abstract><p>В работе представлены результаты исследования электро- и магнетосопротивления композитного материала, состоящего из 70 % мол. дираковского полуметалла Cd3As2 и 30 % мол. ферромагнетика MnAs, при давлениях до 50 ГПа, а также намагниченности при гидростатических давлениях до 6 ГПа в режиме комнатных температур и в интервале 180 – 350 К при атмосферном давлении. В качестве среды, передающей давление, использовали смесь метанола с этанолом в соотношении 4:1. Элементный анализ композитов Cd3As2 + 30 % мол. MnAs показал, что большая часть объема составляет фаза Cd3As2, доля включений фазы MnAs — менее 5 %. Присутствует также значительная область несмешивания расплавов фаз Cd3As2 и MnAs. Установлено, что при увеличении давления во всей исследованной барической области наблюдается отрицательное магнетосопротивление материала (максимум — при 22 – 26 ГПа). При дальнейшем росте давления до максимального уровня на кривой появляются несколько экстремумов, при этом отрицательное магнетосопротивление не превышает 4 %. В режиме сброса давления от 50 ГПа отрицательное магнетосопротивление сменяется положительным (при 40 ГПа), и в районе 20 ГПа наблюдается максимальное значение положительного магнетосопротивления (~5,3 %). Выявлены признаки нестабильности моноклинной структуры Cd3As2 в результате ее частичного разложения при декомпрессии. Полученные результаты могут быть использованы в спинтронике при применении соответствующих композитных материалов.</p></abstract><trans-abstract xml:lang="en"><p>We report on the main results of studying the electrical and magnetoresistance (MR) of a composite material consisting of 70 % mol. Dirac semi-metal Cd3As2 and 30 % mol. ferromagnet MnAs at pressures up to 50 GPa in a diamond anvil cell with a «rounded cone-flat» type anvils, as well as magnetization at hydrostatic pressures up to 6 GPa in a toroid-shaped high-pressure cell, both at room temperature and in the temperature range of 180 – 350 K at atmospheric pressure. A mixture of methanol and ethanol in a ratio of 4:1 was used as a pressure transmitting medium. Elemental analysis of Cd3As2 + 30 % mol MnAs composites showed that much of the volume is occupied by the Cd3As2 phase. The proportion of MnAs phase inclusions is less than 5 %. The feature of Cd3As2 + MnAs is the presence of a significant region of non-mixing of the Cd3As2 and MnAs phase melts. A negative MR was revealed with increasing pressure in the entire studied baric zone. The maximum negative MR is observed in the baric zone of 22 – 26 GPa. Further increase in the pressure up to the maximum level result in the appearance of several extrema on the ΔR/R0(P) curve, with negative MR not exceeding 4 %. Upon pressure release from 50 GPa, the baric dependence of ΔR/R0(P) is characterized by an inversion of the MR sign: at pressures around 40 GPa, a negative MR is replaced by a positive MR, and at around 20 GPa, the maximum value of positive MR of ~5.3 % is observed. Signs of the instability of the monoclinic structure of Cd3As2 resulted from its partial decomposition upon decompression were revealed. The results obtained can be used in spintronics when using appropriate composite materials.</p></trans-abstract><kwd-group xml:lang="ru"><kwd>дираковский полуметалл Cd3As2</kwd><kwd>наногранулы</kwd><kwd>магнетосопротивление</kwd><kwd>ферромагнетик MnAs</kwd></kwd-group><kwd-group xml:lang="en"><kwd>Dirac semimetal Cd3As2</kwd><kwd>nanogranules</kwd><kwd>magnetoresistance</kwd><kwd>MnAs ferromagnet</kwd></kwd-group><funding-group><funding-statement xml:lang="ru">Работа выполнена при финансовой поддержке Минобрнауки РФ (госзадание «0203-2019-008, тема №46.4).</funding-statement></funding-group></article-meta></front><back><ref-list><title>References</title><ref id="cit1"><label>1</label><citation-alternatives><mixed-citation xml:lang="ru">Wang Z., Weng H., Wu Q., et al. Three-dimensional Dirac semimetal and quantum transport in Cd3As2 / Phys. Rev. 2013. Vol. 88. N 12. P. 125427. 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