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<article article-type="research-article" dtd-version="1.3" xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance" xml:lang="ru"><front><journal-meta><journal-id journal-id-type="publisher-id">zldm</journal-id><journal-title-group><journal-title xml:lang="ru">Заводская лаборатория. Диагностика материалов</journal-title><trans-title-group xml:lang="en"><trans-title>Industrial laboratory. Diagnostics of materials</trans-title></trans-title-group></journal-title-group><issn pub-type="ppub">1028-6861</issn><issn pub-type="epub">2588-0187</issn><publisher><publisher-name>ООО «Издательство «ТЕСТ-ЗЛ»</publisher-name></publisher></journal-meta><article-meta><article-id pub-id-type="doi">10.26896/1028-6861-2026-92-6-17-23</article-id><article-id custom-type="elpub" pub-id-type="custom">zldm-2854</article-id><article-categories><subj-group subj-group-type="heading"><subject>Research Article</subject></subj-group><subj-group subj-group-type="section-heading" xml:lang="ru"><subject>АНАЛИЗ ВЕЩЕСТВА</subject></subj-group><subj-group subj-group-type="section-heading" xml:lang="en"><subject>SUBSTANCES ANALYSIS</subject></subj-group></article-categories><title-group><article-title>Использование метода синхронного сканирования спектров флуоресценции для идентификации подлинности пива и пивных напитков</article-title><trans-title-group xml:lang="en"><trans-title>Application of synchronous fluorescence scanning for authenticity identification of beer and beer-based drinks</trans-title></trans-title-group></title-group><contrib-group><contrib contrib-type="author" corresp="yes"><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Васильев</surname><given-names>В. А.</given-names></name><name name-style="western" xml:lang="en"><surname>Vasilyev</surname><given-names>V. A.</given-names></name></name-alternatives><bio xml:lang="ru"><p>Владимир Анатольевич Васильев </p><p>414056, г. Астрахань, ул. Татищева, стр. 16/1.</p></bio><bio xml:lang="en"><p>Vladimir A. Vasilyev </p><p>16/1, Tatishcheva ul., Astrakhan, 414056</p></bio><xref ref-type="aff" rid="aff-1"/></contrib><contrib contrib-type="author" corresp="yes"><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Очередко</surname><given-names>Ю. А.</given-names></name><name name-style="western" xml:lang="en"><surname>Ocheredko</surname><given-names>Yu. A.</given-names></name></name-alternatives><bio xml:lang="ru"><p>Юлия Александровна Очередко</p><p>414056, г. Астрахань, ул. Татищева, д. 20а; 414000, г. Астрахань, ул. Бакинская, д. 121.</p></bio><bio xml:lang="en"><p>Yuliya A. Ocheredko</p><p>20a, Tatishcheva ul., Astrakhan, 414056; 121, Bakinskaya ul., Astrakhan, 414056</p></bio><xref ref-type="aff" rid="aff-2"/></contrib><contrib contrib-type="author" corresp="yes"><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Реснянская</surname><given-names>A. С.</given-names></name><name name-style="western" xml:lang="en"><surname>Resnyanskaya</surname><given-names>A. S.</given-names></name></name-alternatives><bio xml:lang="ru"><p>Анна Станиславовна Реснянская </p><p>414056, г. Астрахань, ул. Татищева, д. 20а.</p></bio><bio xml:lang="en"><p>Anna S. Resnyanskaya</p><p>20a, Tatishcheva ul., Astrakhan, 414056</p><p> </p></bio><email xlink:type="simple">resnyanskaya-as@yandex.ru</email><xref ref-type="aff" rid="aff-3"/></contrib></contrib-group><aff-alternatives id="aff-1"><aff xml:lang="ru"><institution>Астраханский государственный технический университет</institution><country>Россия</country></aff><aff xml:lang="en"><institution>Astrakhan State Technical University</institution><country>Russian Federation</country></aff></aff-alternatives><aff-alternatives id="aff-2"><aff xml:lang="ru"><institution>Астраханский государственный университет им. В. Н. Татищева; &#13;
Астраханский государственный медицинский университет</institution><country>Россия</country></aff><aff xml:lang="en"><institution>Astrakhan Tatishchev State University; &#13;
Astrakhan State Medical University</institution><country>Russian Federation</country></aff></aff-alternatives><aff-alternatives id="aff-3"><aff xml:lang="ru"><institution>Астраханский государственный университет им. В. Н. Татищева</institution><country>Россия</country></aff><aff xml:lang="en"><institution>Astrakhan Tatishchev State University</institution><country>Russian Federation</country></aff></aff-alternatives><pub-date pub-type="collection"><year>2026</year></pub-date><pub-date pub-type="epub"><day>04</day><month>07</month><year>2026</year></pub-date><volume>92</volume><issue>6</issue><fpage>17</fpage><lpage>23</lpage><permissions><copyright-statement>Copyright &amp;#x00A9; Васильев В.А., Очередко Ю.А., Реснянская A.С., 2026</copyright-statement><copyright-year>2026</copyright-year><copyright-holder xml:lang="ru">Васильев В.А., Очередко Ю.А., Реснянская A.С.</copyright-holder><copyright-holder xml:lang="en">Vasilyev V.A., Ocheredko Y.A., Resnyanskaya A.S.</copyright-holder><license xml:lang="ru" license-type="creative-commons-attribution" xlink:href="https://creativecommons.org/licenses/by/4.0/" xlink:type="simple"><license-p>Данная работа распространяется под лицензией Creative Commons Attribution 4.0.</license-p></license><license xml:lang="en" license-type="creative-commons-attribution" xlink:href="https://creativecommons.org/licenses/by/4.0/" xlink:type="simple"><license-p>This work is licensed under a Creative Commons Attribution 4.0 License.</license-p></license></permissions><self-uri xlink:href="https://www.zldm.ru/jour/article/view/2854">https://www.zldm.ru/jour/article/view/2854</self-uri><abstract><p>В связи с усилением государственного контроля производства и оборота крепких спиртных напитков фальсификации все чаще подвергается алкогольная продукция, не подлежащая обязательному лицензированию, прежде всего пиво и пивные напитки. В целях контроля их качества провели синхронное сканирование спектров флуоресценции четырех образцов пива и пятнадцати образцов пивных напитков с использованием двухлучевого спектрофотометра-флуориметра СФФ-2 «Флуоран». Чтобы обеспечить наибольшую информативность полученных спектров при наименьших временных затратах, варьировали диапазоны длин волн испускания и возбуждения, а также их разность. Синхронное сканирование подлинных и фальсифицированных образцов проводили в диапазоне длин волн 250 – 600 нм при разности длин волн возбуждения и эмиссии Δλ = 30 и 60 нм. В спектрах натурального пива и пивных напитков отчетливо присутствуют максимумы высокой интенсивности в коротковолновой области на длинах волн 280 (Δλ = 30 нм) и 275 нм (Δλ = 60 нм) и минимум λ = 313 нм, а также длинноволновые максимумы λ = 362 (Δλ = 30 нм) и 336 нм (Δλ = 60 нм). В случае фальсифицированных образцов положение длинноволнового максимума не изменилось. Анализ полученных данных показал, что часть образцов пивных напитков и пива имеет характеристические отклики присутствующих в них маркерных флуоресцирующих соединений, что позволяет отнести эти образцы к подлинным, тогда как отсутствие или значительно более низкая интенсивность сигналов этих соединений в спектре ряда других образцов свидетельствует об их фальсификации. Показано, что образцы пива, принадлежащие к одной партии, но реализуемые в разных регионах, имеют очень близкие флуоресцентные характеристики. Данный метод можно использовать для оперативного выявления фальсификатов пивной продукции.</p></abstract><trans-abstract xml:lang="en"><p>Due to increased state control over the production and circulation of distilled spirits, alcoholic products that do not comply with mandatory licensing, primarily beer and beer beverages are increasingly being adulterated. For their quality control the application of synchronous fluorescence scanning spectroscopy is described. Four beer samples and fifteen beer beverage samples were investigated. A double-beam spectrophotometer-fluorimeter SFF-2 «Fluoran» was used for the measurements. To optimize the parameters ensuring the highest information content of the obtained spectra with minimal time expenditure, the wavelength ranges of emission and excitation, their difference (Δλ), and instrument settings were varied during the experiments. Synchronous scanning of authentic and adulterated samples was performed in the wavelength range of 250 – 600 nm at wavelength differences between excitation and emission of Δλ = 30 and 60 nm. The synchronous scanning spectra of genuine beer and beer beverages clearly exhibit high-intensity maxima in the short-wavelength region at 280 (Δλ = 30 nm) and 275 nm (Δλ = 60 nm), as well as a distinct minimum at λ = 313 nm. The long-wavelength maximum was observed at 362 (Δλ = 30 nm) and 336 nm (Δλ = 60 nm). In the adulterated samples, the position of the long-wavelength maximum remained unchanged. Analysis of the obtained data showed that some beer beverage and beer samples exhibit characteristic responses from marker fluorescent compounds present in them. Other samples either lack such responses or show significantly lower intensity. It was also demonstrated that beer samples from the same batch but sold in different regions have very similar fluorescence characteristics. This method can be used for the rapid detection of adulterated products; however, further research is needed to accumulate a statistically significant dataset.</p></trans-abstract><kwd-group xml:lang="ru"><kwd>синхронная флуоресцентная спектроскопия</kwd><kwd>пиво</kwd><kwd>пивные напитки</kwd><kwd>фальсификация</kwd><kwd>идентификации подлинности</kwd><kwd>идентичность образцов</kwd></kwd-group><kwd-group xml:lang="en"><kwd>synchronous fluorescence spectroscopy</kwd><kwd>beer</kwd><kwd>beer beverages</kwd><kwd>adulteration</kwd><kwd>authenticity identification</kwd><kwd>sample identity</kwd></kwd-group></article-meta></front><back><ref-list><title>References</title><ref id="cit1"><label>1</label><citation-alternatives><mixed-citation xml:lang="ru">Khurshudyan S. A., Zakharov M. A., Obodeeva O. N., Ul’yanova E. V. Fermentation beverages: verification of authenticity by chromatographic analysis / Prod. Qual. Control. 2020. No. 7. P. 49 – 52 [in Russian]. 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