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<article article-type="research-article" dtd-version="1.3" xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance" xml:lang="ru"><front><journal-meta><journal-id journal-id-type="publisher-id">zldm</journal-id><journal-title-group><journal-title xml:lang="ru">Заводская лаборатория. Диагностика материалов</journal-title><trans-title-group xml:lang="en"><trans-title>Industrial laboratory. Diagnostics of materials</trans-title></trans-title-group></journal-title-group><issn pub-type="ppub">1028-6861</issn><issn pub-type="epub">2588-0187</issn><publisher><publisher-name>ООО «Издательство «ТЕСТ-ЗЛ»</publisher-name></publisher></journal-meta><article-meta><article-id custom-type="elpub" pub-id-type="custom">zldm-536</article-id><article-categories><subj-group subj-group-type="heading"><subject>Research Article</subject></subj-group><subj-group subj-group-type="section-heading" xml:lang="ru"><subject>МЕХАНИКА МАТЕРИАЛОВ: ПРОЧНОСТЬ, РЕСУРС, БЕЗОПАСНОСТЬ</subject></subj-group><subj-group subj-group-type="section-heading" xml:lang="en"><subject>MECHANICAL TESTING METHODS</subject></subj-group></article-categories><title-group><article-title>Особенности определения твердости и трещиностойкости твердых сплавов при разных нагрузках вдавливания пирамиды</article-title><trans-title-group xml:lang="en"><trans-title>Features of Hardness and Crack Resistance Determination in Hard Alloys under Different Loading of Indenting Pyramid</trans-title></trans-title-group></title-group><contrib-group><contrib contrib-type="author" corresp="yes"><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Дворник</surname><given-names>М. И.</given-names></name><name name-style="western" xml:lang="en"><surname>Dvornik</surname><given-names>M. I.</given-names></name></name-alternatives><email xlink:type="simple">secretar@im.febras.net. infarest@infarest.khv.ru</email><xref ref-type="aff" rid="aff-1"/></contrib><contrib contrib-type="author" corresp="yes"><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Ершова</surname><given-names>Т. Б.</given-names></name><name name-style="western" xml:lang="en"><surname>Ershova</surname><given-names>T. B.</given-names></name></name-alternatives><email xlink:type="simple">secretar@im.febras.net. infarest@infarest.khv.ru</email><xref ref-type="aff" rid="aff-1"/></contrib><contrib contrib-type="author" corresp="yes"><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Михайленко</surname><given-names>Е. А.</given-names></name><name name-style="western" xml:lang="en"><surname>Mikhailenko</surname><given-names>E. A.</given-names></name></name-alternatives><email xlink:type="simple">secretar@im.febras.net. infarest@infarest.khv.ru</email><xref ref-type="aff" rid="aff-1"/></contrib><contrib contrib-type="author" corresp="yes"><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Крутикова</surname><given-names>В. О.</given-names></name><name name-style="western" xml:lang="en"><surname>Krutikova</surname><given-names>V. O.</given-names></name></name-alternatives><email xlink:type="simple">nick@itig.as.khb.ru</email><xref ref-type="aff" rid="aff-2"/></contrib></contrib-group><aff xml:lang="ru" id="aff-1"><institution>Институт материаловедения Хабаровского научного центра ДВО РАН</institution><country>Russian Federation</country></aff><aff xml:lang="ru" id="aff-2"><institution>Институт тектоники и геофизики ДВО РАН</institution><country>Russian Federation</country></aff><pub-date pub-type="collection"><year>2017</year></pub-date><pub-date pub-type="epub"><day>01</day><month>09</month><year>2017</year></pub-date><volume>83</volume><issue>9</issue><fpage>57</fpage><lpage>65</lpage><permissions><copyright-statement>Copyright &amp;#x00A9; Дворник М.И., Ершова Т.Б., Михайленко Е.А., Крутикова В.О., 2017</copyright-statement><copyright-year>2017</copyright-year><copyright-holder xml:lang="ru">Дворник М.И., Ершова Т.Б., Михайленко Е.А., Крутикова В.О.</copyright-holder><copyright-holder xml:lang="en">Dvornik M.I., Ershova T.B., Mikhailenko E.A., Krutikova V.O.</copyright-holder><license xml:lang="ru" license-type="creative-commons-attribution" xlink:href="https://creativecommons.org/licenses/by/4.0/" xlink:type="simple"><license-p>Данная работа распространяется под лицензией Creative Commons Attribution 4.0.</license-p></license><license xml:lang="en" license-type="creative-commons-attribution" xlink:href="https://creativecommons.org/licenses/by/4.0/" xlink:type="simple"><license-p>This work is licensed under a Creative Commons Attribution 4.0 License.</license-p></license></permissions><self-uri xlink:href="https://www.zldm.ru/jour/article/view/536">https://www.zldm.ru/jour/article/view/536</self-uri><abstract><p>Рассмотрен размерный эффект, возникающий при уменьшении нагрузки с 50 до 0,05 кгс в процессе измерения твердости по Виккерсу среднезернистого (WC-8Co), субмикронного (WC-8Co-1Cr3C2) и ультрамелкозернистого (WC-8Co-0,4VC-0,4Cr3C2) твердых сплавов, а также стандартных твердых сплавов ВК6ОМ и Т15К6. Прирост твердости в результате размерного эффекта достигает 14 - 16 %. Показано, что возле отпечатков твердомера возникают возвышения, которые искажают результаты измерений. Установлено наличие обратной зависимости твердости от размера отпечатка индентора. Наибольший размерный эффект наблюдается у более твердого ультрамелкозернистого сплава. Проведено сравнение результатов измерения трещиностойкости методом Палмквиста с помощью оптического и растрового микроскопов. Отмечено, что формирование трещин по схеме Палмквиста происходит под воздействием нагрузок, превышающих определенную величину, которая зависит от трещиностойкости сплава. Отжиг не оказывает значительного влияния на результаты измерения твердости и трещиностойкости. Полученные результаты подтверждают снижение трещиностойкости при повышении твердости за счет уменьшения среднего размера зерна WC при переходе от среднезернистых твердых сплавов к субмикронным и ультрамелкозернистым сплавам.</p></abstract><trans-abstract xml:lang="en"><p>The size effect arising upon the load decrease from 50 kgf up to 0.05 kgf in measurements of the Vickers hardness for medium-grained (WC-8Co), submicron (WC-8Co-1Cr3C2) and ultrafine-grained (WC-8Co-0.4VC-0.4Cr3C2) hard alloys, as well as standard hard alloys T15K6 and VK6OM is considered. An increase in hardness resulting from the size effect attains 14 - 16%. Presence of the elevations near the penetrator indentation distorts the measurement results. The inverse dependence of hardness on the size of indentation is demonstrated. The largest dimensional effect is observed for the hardest ultrafine-grained alloy. The results of the fracture resistance measurements using Palmquist method for optical and raster microscopes are compared. It is shown that crack formation in the Palmquist scheme occurs under the impact of loads exceeding a critical value, which depends on the fracture toughness of the alloy. Annealing does not have a significant effect on the results of hardness and fracture toughness measurements. The results confirm a decrease in the crack resistance with increasing hardness due to reduction in the average grain size of WC sample when going from medium-grained hard alloys to submicron and ultrafine-grained alloys.</p></trans-abstract><kwd-group xml:lang="ru"><kwd>твердость Виккерса</kwd><kwd>трещиностойкость Палмквиста</kwd><kwd>индентирование</kwd><kwd>размерный эффект</kwd><kwd>ультрамелкозернистый твердый сплав</kwd><kwd>Vickers hardness</kwd><kwd>Palmquist crack toughness</kwd><kwd>indentation</kwd><kwd>size effect</kwd><kwd>ultrafine hard alloy</kwd></kwd-group></article-meta></front><back><ref-list><title>References</title><ref id="cit1"><label>1</label><citation-alternatives><mixed-citation xml:lang="ru">Liu Xuemei, Song Xiaoyan, Zhang Jiuxing, Zhao Shixian. Temperature distribution and neck formation of WC-Co combined particles during spark plasma sintering / Mater. Sci. Engin. A. 2008. Vol. 488. 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