<?xml version="1.0" encoding="UTF-8"?>
<!DOCTYPE article PUBLIC "-//NLM//DTD JATS (Z39.96) Journal Publishing DTD v1.3 20210610//EN" "JATS-journalpublishing1-3.dtd">
<article article-type="research-article" dtd-version="1.3" xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance" xml:lang="ru"><front><journal-meta><journal-id journal-id-type="publisher-id">zldm</journal-id><journal-title-group><journal-title xml:lang="ru">Заводская лаборатория. Диагностика материалов</journal-title><trans-title-group xml:lang="en"><trans-title>Industrial laboratory. Diagnostics of materials</trans-title></trans-title-group></journal-title-group><issn pub-type="ppub">1028-6861</issn><issn pub-type="epub">2588-0187</issn><publisher><publisher-name>ООО «Издательство «ТЕСТ-ЗЛ»</publisher-name></publisher></journal-meta><article-meta><article-id pub-id-type="doi">10.26896/1028-6861-2019-85-2-29-32</article-id><article-id custom-type="elpub" pub-id-type="custom">zldm-910</article-id><article-categories><subj-group subj-group-type="heading"><subject>Research Article</subject></subj-group><subj-group subj-group-type="section-heading" xml:lang="ru"><subject>ИССЛЕДОВАНИЕ СТРУКТУРЫ И СВОЙСТВ. ФИЗИЧЕСКИЕ МЕТОДЫ ИССЛЕДОВАНИЯ И КОНТРОЛЯ</subject></subj-group><subj-group subj-group-type="section-heading" xml:lang="en"><subject>TESTING OF STRUCTURE AND PARAMETERS. PHYSICAL METHODS OF TESTING AND QUALITY CONTROL</subject></subj-group></article-categories><title-group><article-title>Определение ориентации внутренних линейных дефектов в изотропных оптических кристаллах</article-title><trans-title-group xml:lang="en"><trans-title>Determination of the orientation of internal linear defects in isotropic optical crystals</trans-title></trans-title-group></title-group><contrib-group><contrib contrib-type="author" corresp="yes"><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Чередов</surname><given-names>В. Н.</given-names></name><name name-style="western" xml:lang="en"><surname>Cheredov</surname><given-names>V. N.</given-names></name></name-alternatives><bio xml:lang="ru"><p>Валерий Николаевич Чередов</p></bio><bio xml:lang="en"/><email xlink:type="simple">cvn@rambler.ru</email><xref ref-type="aff" rid="aff-1"/></contrib><contrib contrib-type="author" corresp="yes"><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Петраков</surname><given-names>А. П.</given-names></name><name name-style="western" xml:lang="en"><surname>Petrakov</surname><given-names>A. E.</given-names></name></name-alternatives><bio xml:lang="ru"/><bio xml:lang="en"/><email xlink:type="simple">cvn@rambler.ru</email><xref ref-type="aff" rid="aff-1"/></contrib></contrib-group><aff-alternatives id="aff-1"><aff xml:lang="ru"><institution>Сыктывкарский государственный университет</institution><country>Россия</country></aff><aff xml:lang="en"><institution>Syktyvkar State University</institution><country>Russian Federation</country></aff></aff-alternatives><pub-date pub-type="collection"><year>2019</year></pub-date><pub-date pub-type="epub"><day>28</day><month>02</month><year>2019</year></pub-date><volume>85</volume><issue>2</issue><fpage>29</fpage><lpage>32</lpage><permissions><copyright-statement>Copyright &amp;#x00A9; Чередов В.Н., Петраков А.П., 2019</copyright-statement><copyright-year>2019</copyright-year><copyright-holder xml:lang="ru">Чередов В.Н., Петраков А.П.</copyright-holder><copyright-holder xml:lang="en">Cheredov V.N., Petrakov A.E.</copyright-holder><license xml:lang="ru" license-type="creative-commons-attribution" xlink:href="https://creativecommons.org/licenses/by/4.0/" xlink:type="simple"><license-p>Данная работа распространяется под лицензией Creative Commons Attribution 4.0.</license-p></license><license xml:lang="en" license-type="creative-commons-attribution" xlink:href="https://creativecommons.org/licenses/by/4.0/" xlink:type="simple"><license-p>This work is licensed under a Creative Commons Attribution 4.0 License.</license-p></license></permissions><self-uri xlink:href="https://www.zldm.ru/jour/article/view/910">https://www.zldm.ru/jour/article/view/910</self-uri><abstract><p>Исследование структуры оптических кристаллов и дефектов в них — одна из важнейших задач кристаллофизики, кристаллографии и материаловедения. В последние годы, как известно, возрос интерес к линейным дефектам в кристаллах, которые (прежде всего линейные несовершенства кристаллической структуры) существенно снижают эксплуатационные физические свойства оптических кристаллов. Представлен способ экспрессного определения кристаллографической ориентации линейных дефектов (дислокаций, их скоплений, линейно вытянутых объемных включений и др.) в оптических кристаллах. Ориентацию линейно вытянутой микропоры в изотропном оптическом прозрачном кристалле флюорита определяли с использованием оптического микроскопа. Вращая кристалл, закрепленный в кристаплодержателе микроскопа, фиксировали показания шкапы барабана окуляра. Поправки на преломление света в объеме кристалла учитывали аналитически. Кристаллографические индексы ориентации микропоры соответствовали [<xref ref-type="bibr" rid="cit100">100</xref>]. Приведены зависящие от значения показателя преломления ограничения на углы поворота кристалла, используемые при данном способе определения ориентации линейного дефекта.</p></abstract><trans-abstract xml:lang="en"><p>Study of the structure of optical crystals and defects in them is one of the most important problems in crystal physics, crystallography and material science. Nowadays, study of the nanostructures, including the linear defects in crystals is of particular importance. Defects, and first and foremost linear imperfections of the crystal structure, significantly reduce the operational physical properties of optical crystals. Analysis of the properties of those defects, their orientation in the crystal lattice, as well as developing of the methods for determination of the crystallographic orientation of linear defects are the most important in view of the possibility of improving the properties of optical crystals. A method for rapid determination of the crystallographic orientation of linear defects (dislocations, clusters, linearly extended bulk inclusions, etc.) in optical crystals is presented. The orientation of a linearly extended micropore in an isotropic optical transparent fluorite crystal was determined using an optical microscope. The readings of the scale of the eyepiece drum were recorded when rotating the crystal fixed in the crystal holder of the microscope. Corrections for the refraction of light in the bulk of the crystal were taken into account analytically. The crystallographic orientation of the microporous in a transparent fluorite crystal was studied in detail. Crystallographic indices of micropore orientation corresponded to [<xref ref-type="bibr" rid="cit100">100</xref>]. We developed an efficient rapid procedure for determination of the orientation of internal linear defects (imperfections) in optically isotropic crystals using an optical microscope. The restrictions imposed on the angles of crystal rotation depending on the value of the refractive index are considered for the given method of determination.</p></trans-abstract><kwd-group xml:lang="ru"><kwd>линейные дефекты</kwd><kwd>изотропные оптические кристаллы</kwd><kwd>способ определения кристаллографической ориентации</kwd></kwd-group><kwd-group xml:lang="en"><kwd>linear defects</kwd><kwd>isotropic optical crystals</kwd><kwd>method for determination of crystallographic orientation</kwd></kwd-group></article-meta></front><back><ref-list><title>References</title><ref id="cit1"><label>1</label><citation-alternatives><mixed-citation xml:lang="ru">Doherty М., Miehl J., Dolde F., et al. Measuring the defect structure orientation of a single NV-centre in diamond / New J. Phys. 2014. Vol. 16. P 1 - 20.</mixed-citation><mixed-citation xml:lang="en">Doherty M., Miehl J., Dolde F., et al. Measuring the defect structure orientation of a single NV-centre in diamond / New J. Phys. 2014. Vol. 16. E 1 - 20.</mixed-citation></citation-alternatives></ref><ref id="cit2"><label>2</label><citation-alternatives><mixed-citation xml:lang="ru">A. c. 949434 СССР. Способ определения кристаллографической ориентации внутренних несовершенств прозрачных кристаллов / Белянин А. Ф., Бульенков Н. А. — № 2951031; заявл. 30.06.1980; опубл. 07.08.1982. Бюл. № 29.</mixed-citation><mixed-citation xml:lang="en">USSR Inventor’s Certificate 949434. Method for determining the crystallographic orientation of internal imperfections of transparent crystals / Belyanin A. F., Bulenkov N. A. — N2951031; appl. 30.06.1980; publ. 07.08.1982. Byull. N29 [in Russian].</mixed-citation></citation-alternatives></ref><ref id="cit3"><label>3</label><citation-alternatives><mixed-citation xml:lang="ru">А. с. 1000477 СССР. Способ определения кристаллографической ориентации монокристаллов с ОЦК-решеткой / Измаилов Ф. И. — № 3271374; заявл. 01.04.1981; опубл. 28.02.1983. Бюл. № 8.</mixed-citation><mixed-citation xml:lang="en">USSR Inventor’s Certificate 1000477 USSR. The method for determining the crystallographic orientation of single crystals with a bcc lattice / Izmailov EL — N 3271374; appl. 01.04.1981; publ. 28.02.1983. Byull. N 8 [in Russian],</mixed-citation></citation-alternatives></ref><ref id="cit4"><label>4</label><citation-alternatives><mixed-citation xml:lang="ru">А. с. 1522027 СССР. Способ определения ориентации монокристаллов / Чередов В. Н. — № 4258229; заявл. 08.06.1987; опубл. 15.11.1989. Бюл. № 42.</mixed-citation><mixed-citation xml:lang="en">USSR Inventor’s Certificate 1522027 USSR. Method for determining the orientation of single crystals / Cheredov V N. — N4258229; appl. 08.06.1987; publ. 15.11.1989. Bull. N42 [in Russian].</mixed-citation></citation-alternatives></ref><ref id="cit5"><label>5</label><citation-alternatives><mixed-citation xml:lang="ru">А. с. 890179 СССР. Дифрактометрический способ определения ориентировки монокристаллов / Фомин В. Г., Новиков А. Г., Освенский В. Б., Утенкова О. В. — № 2916621; заявл. 25.04.1980; опубл. 15.12.1981. Бюл. № 46.</mixed-citation><mixed-citation xml:lang="en">USSR Inventor’s Certificate 890179. Diffractometric method for determining the orientation of single crystals / Fomin V G., Novikov A. G., Osvensky V B., Utenkova О. V — N 2916621; appl. 25.04.1980; publ. 15.12.1981. Byull. N 46 [in Russian],</mixed-citation></citation-alternatives></ref><ref id="cit6"><label>6</label><citation-alternatives><mixed-citation xml:lang="ru">Борн М., Вольф Э. Основы оптики. — М.: Наука, 1973. — 720 с.</mixed-citation><mixed-citation xml:lang="en">Born M., Wolf E. Foundations of Optics. — Moscow: Nauka, 1973. — 720 p. [in Russian],</mixed-citation></citation-alternatives></ref><ref id="cit7"><label>7</label><citation-alternatives><mixed-citation xml:lang="ru">Корн Г., Корн Т. Справочник по математике. — М.: Наука, 1978.—832 с.</mixed-citation><mixed-citation xml:lang="en">Korn G., Korn T. Handbook of Mathematics. — Moscow: Nauka, 1978. — 832 p. [in Russian],</mixed-citation></citation-alternatives></ref><ref id="cit8"><label>8</label><citation-alternatives><mixed-citation xml:lang="ru">Бабичева И. Е., Болдовекая Т. Е. Справочник по математике (в формулах, таблицах, рисунках). — Омск: СибАДИ, 2010.— 148 с.</mixed-citation><mixed-citation xml:lang="en">Babicheva I. E., Boldovskaya T. E. Reference book on mathematics (in formulas, tables, figures). — Omsk: SibADI, 2010. — 148 p. [in Russian],</mixed-citation></citation-alternatives></ref><ref id="cit9"><label>9</label><citation-alternatives><mixed-citation xml:lang="ru">Dowty Е. Computing and drawing crystal shapes / The American Mineralogist. 1980. Vol. 65. N 5. P 465 - 471.</mixed-citation><mixed-citation xml:lang="en">Dowty E. Computing and drawing crystal shapes / The American Mineralogist. 1980. Vol. 65. N 5. E 465 — 471.</mixed-citation></citation-alternatives></ref></ref-list><fn-group><fn fn-type="conflict"><p>The authors declare that there are no conflicts of interest present.</p></fn></fn-group></back></article>
