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Study of the anisotropy of the properties of the ceramic cutting insert obtained by the LCM technology of 3D printing from the composite Al2O3/ZrO2 (ZTA)

https://doi.org/10.26896/1028-6861-2021-87-11-64-69

Abstract

The anisotropy of the properties of a ceramic cutting insert (for three faces) obtained by the lithography-based technology from the Al2O3 + ZrO2 composite has been studied. The study was carried out using the indentation method and Mayer’s law. This method, in contrast to the bending test, excludes the sample destruction. All the studies were carried out on three faces of a ceramic cutting insert made of a composite Al2O3 + ZrO2. The behavior of the Mayer index was studied in the range of loads from 2 to 20 kg and from 0.2 to 1 kg. The results of studying the density, phase composition and microstructure of each face of the sample are presented. The study of the adhesion of the printed layers were also carried out using a Knoop indenter. No anisotropy of the hardness was observed in the load range up to 10 kg. It is shown that a layered structure present in the sample, contributes to the hardness anisotropy under the load of 20 kg and more. No anisotropy of the fracture toughness is observed in the load range of 2 – 20 kg. The results of using a Knoop indenter revealed a high adhesion between 3D printed layers. Studies using a Knoop indenter have indicated high adhesion between the layers of 3D printing.

About the Authors

G. V. Shcherbak
N.I. Lobachevsky Nizhni Novgorod State University
Russian Federation

Gleb V. Shcherbak

23, prosp. Gagarina, Nizhny Novgorod, 603022



A. A. Murashov
N.I. Lobachevsky Nizhni Novgorod State University
Russian Federation

Artem A. Murashov

23, prosp. Gagarina, Nizhny Novgorod, 603022



K. E. Smetanina
N.I. Lobachevsky Nizhni Novgorod State University
Russian Federation

Kseniya E. Smetanina

23, prosp. Gagarina, Nizhny Novgorod, 603022



M. M. Vostokov
N.I. Lobachevsky Nizhni Novgorod State University
Russian Federation

Mikhail M. Vostokov

23, prosp. Gagarina, Nizhny Novgorod, 603022



M. S. Boldin
N.I. Lobachevsky Nizhni Novgorod State University
Russian Federation

Maksim S. Boldin

23, prosp. Gagarina, Nizhny Novgorod, 603022



References

1. Denry I., Robert Kelly J. State of the art of zirconia for dental applications / Dental Mater. 2008. Vol. 24. P. 299 – 307. DOI: 10.1016/j.dental.2007.05.007

2. Zadorozhnaya O. Yu., Tiunova O. V., Bogaev A. A., et al. The influence of both nano-sized ZrO2 additions and the compression process operational conditions on the Al2O3 and ZrO2 composites properties / Nov. Ogneupory. 2013. N 10. P. 21 – 26 [in Russian].

3. Matrenin S. V., Slosman A. I. Technical ceramics. — Tomsk: Izd. TPU, 2004. — 75 p. [in Russian].

4. Altun A. A., Prochaska T., Konegger T., Schwentenwein M. Dense, Strong, and Precise Silicon Nitride-Based Ceramic Parts by Lithography-Based Ceramic Manufacturing / Appl. Sci. 2020. Vol. 10. Issue 3. N 996. P. 14. DOI: 10.3390/app10030996

5. Moritz T. Additive manufacturing. Fraunhofer Institute for Ceramic Technologies and Systems IKTS. 2020 https://www.ikts.fraunhofer.de/en/industrial_solutions/additive_manufacturing.html

6. Moritz T., Partsch U., Ziesche S., Scheithauer U., Ahlhelm M., Schwarzer E., Richter H. J. Additive manufacturing of ceramic components / Fraunhofer Institute for Ceramic Technologies and Systems IKTS. Annual Report 2014/15. P. 28 – 31. https://www.ikts.fraunhofer.de/content/dam/ikts/downloads/annual reports/jb2014/Fraunhofer_IKTS_2014_Annual_Report.pdf

7. Homa J. Relating Ceramic Mechanical Properties Standards to Advanced Ceramics Produced by LCM. Webinar Lithoz GmbH. 2020. https://www.youtube.com/watch?v=ZPkdrU9m8Tw

8. McColm I. J. Ceramic hardness. — New York: Springer Science and Business Media, 1990. P. 324. DOI: 10.1007/978-1-4757-4732-4

9. Jianghong G., Jianjun W., Zhenduo G. Examination of the Indentation Size Effect in Low-load Vickers Hardness Testing of Ceramics / J. Eur. Ceram. Soc. 1999. Vol. 19. Issue 15. P. 2625 – 2631. DOI: 10.1016/S0955-2219(99)00043-6

10. Quinn J. B., Quinn G. D. Indentation brittleness of ceramics: a fresh approach / J. Mater. Sci. 1997. Vol. 32. Issue 16. P. 4331 – 4346. DOI: 10.1023/A:1018671823059


Review

For citations:


Shcherbak G.V., Murashov A.A., Smetanina K.E., Vostokov M.M., Boldin M.S. Study of the anisotropy of the properties of the ceramic cutting insert obtained by the LCM technology of 3D printing from the composite Al2O3/ZrO2 (ZTA). Industrial laboratory. Diagnostics of materials. 2021;87(11):64-69. (In Russ.) https://doi.org/10.26896/1028-6861-2021-87-11-64-69

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ISSN 1028-6861 (Print)
ISSN 2588-0187 (Online)