CURRENT STATE AND PROBLEMS OF ANALYTICAL CONTROL OF WASTE AUTOMOTIVE CATALYSTS (REVIEW)
https://doi.org/10.26896/1028-6861-2017-83-11-5-14
Abstract
Spent autocatalysts hold a specific place among secondary raw materials containing precious metals. Precise determination of platinum metals in spent autocatalysts (SA) plays a very important role affecting the economic efficiency of the utilization process. We generalize the existing methods of analysis of spent autocatalysts presented in the literature and methodological developments of the Institute «Giredmet» in collaboration with the Center «ANSERTECO» and NUST «MISiS» regarding the same problem. The main emphasis is made on the use of modern tools for chemical preparation of hard-to-break object like spent autocatalysts: autoclave and microwave opening of the samples. The advantages of using the assay concentration method based on the developments of the Ekaterinburg Non-Ferrous Metals Processing Plant for analysis of spent autocatalysts are concidered. The atomic emission, atomic absorption and chemical spectroscopic methods of SA analysis have been developed and certified along with the guidelines of their further improvement.
About the Authors
T. Yu. Alekseeva
ООО «АНСЕРТЭКО», Москва;
НИТУ «МИСиС», Москва
Russian Federation
Russian Federation
Yu. A. Karpov
НИТУ «МИСиС», Москва;
АО «Государственный научно-исследовательский и проектный институт редкометаллической промышленности «ГИРЕДМЕТ», Москва;
Институт общей и неорганической химии имени Н. С. Курнакова РАН, Москва
Russian Federation
Russian Federation
O. A. Dalnova
НИТУ «МИСиС», Москва;
АО «Государственный научно-исследовательский и проектный институт редкометаллической промышленности «ГИРЕДМЕТ», Москва
Russian Federation
Russian Federation
V. V. Eskina
НИТУ «МИСиС», Москва;
АО «Государственный научно-исследовательский и проектный институт редкометаллической промышленности «ГИРЕДМЕТ», Москва
Russian Federation
Russian Federation
V. B. Baranovskaya
НИТУ «МИСиС», Москва;
АО «Государственный научно-исследовательский и проектный институт редкометаллической промышленности «ГИРЕДМЕТ», Москва;
Институт общей и неорганической химии имени Н. С. Курнакова РАН, Москва
Russian Federation
Russian Federation
L. D. Gorbatova
АО «Екатеринбургский завод по обработке цветных металлов», г. Верхняя Пышма
Russian Federation
Russian Federation
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Review
For citations:
Alekseeva T.Yu., Karpov Yu.A., Dalnova O.A., Eskina V.V., Baranovskaya V.B., Gorbatova L.D. CURRENT STATE AND PROBLEMS OF ANALYTICAL CONTROL OF WASTE AUTOMOTIVE CATALYSTS (REVIEW). Industrial laboratory. Diagnostics of materials. 2017;83(11):5-14. (In Russ.) https://doi.org/10.26896/1028-6861-2017-83-11-5-14
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