Experience of using atomic-emission spectrometers with MAÉS in an accredited laboratory
https://doi.org/10.26896/1028-6861-2019-85-1-II-33-37
Abstract
A system of the set rules, procedures and regulatory documents is developed in the Central Analytical Laboratory of the JSC «EZ OCM» for the method of atomic emission spectral analysis of precious metals with arc excitation of the spectrum to meet all the requirements of the accrediting body «Rosakkreditatsiya». The features of managing the measuring instruments — spectrometers with MAÉS analyzers, auxiliary equipment and microclimate are considered. The requirements to the personnel of the laboratory for spectral analysis are considered. The rules for developing measurement procedures, instructions for laboratory technicians, measuring programs, methods for performing routine analysis of the samples, and ensuring the traceability of measurement results are specified. The availability of using «ATOM3.3» software for solving everyday problems of the laboratory is shown.
About the Authors
M. D. Lisienko
JSC “Yekaterinburg Non-Ferrous Metals Processing Plant”
Russian Federation
Verkhnyaya Pyshma
Russian Federation
Verkhnyaya Pyshma
N. A. Klimova
JSC “Yekaterinburg Non-Ferrous Metals Processing Plant”
Russian Federation
Verkhnyaya Pyshma
Russian Federation
Verkhnyaya Pyshma
References
1. Plonskiy P. Century of labor victories. 100th anniversary of Yekaterinburg Non-Ferrous Metals Processing Plant — Yekaterinburg: Izd. dom «Sokrat», 2016. — 130 p. [in Russian].
2. Labusov V. A., Garanin V. G., Shelpakova I. R. Multichannel Analyzers of Atomic Emission Spectra: Current State and Analytical Potentials / J. Anal. Chem. 2012. Vol. 67. N 7. P. 632 – 641.
3. ISO/IEC 17025:2005. General requirements for the competence of testing and calibration laboratories.
4. On approval of the Criteria for accreditation, the list of documents confirming the compliance of the applicant, the accredited person with the criteria for accreditation, and the list of documents in the field of standardization, compliance with the requirements of applicants, accredited persons ensures their compliance with the accreditation criteria of May 30, 2014 No. 326: order the Ministry of Economic Development of the Russian Federation [in Russian].
5. On ensuring the uniformity of measurements: Federal Law No. 102-FZ. Adopted 26.06.2008 [in Russian].
6. On the re-measurement instruments, which are verified only by accredited in the established order in the field of ensuring the uniformity of measurements by state regional metrology centers: resolution of the Government of the Russian Federation No. 250 dated 20.04.2010 as amended on October 12, 2017 [in Russian].
7. Petreeva E. Yu., Lisienko D. G., Kurbatova I. B., Lisienko M. D. Analysis of platinum-rhodium alloys using the MAES analyzer / Analit. Kontrol’. 2005. N 2. P. 176 – 181 [in Russian].
8. Kurbatova I. B., Lisienko M. D., Petreeva E. Yu. Development of a unified method for the analysis of platinum-iridium alloys / Analit. Kontrol’. 2005. Vol. 9. N 2. P. 170 – 175 [in Russian].
9. Lisienko D. G., Dombrovskaya M. A. Analyzer MAES in the system of training specialists in the field of atomic emission spectral analysis / Zavod. Lab. Diagn. Mater. 2007. Vol. 73. Special Issue. P. 51 – 53 [in Russian].
10. Anchutina E. A., Gorbatova L. D., Lisienko M. D. Reference materials of JSC «EZ OCM» — past, present, future / Standart. Obr. 2015. N 3. P. 10 – 15 [in Russian].
11. Gorbatova L. D., Anchutina E. A., Lisienko M. D. Reference materials to ensure the reliability of the results of analysis of products from precious metals / Tsvet. met. 2016. N 8. P. 33 – 38 [in Russian].
Review
For citations:
Lisienko M.D., Klimova N.A. Experience of using atomic-emission spectrometers with MAÉS in an accredited laboratory. Industrial laboratory. Diagnostics of materials. 2019;85(1(II)):33-37. (In Russ.) https://doi.org/10.26896/1028-6861-2019-85-1-II-33-37
Views:
612
Email this article 