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DETERMINATION OF ALUMINUM IN STEEL BY INDUCTIVELY COUPLED PLASMA-ATOMIC EMISSION SPECTROMETRY (ICP-AES)

https://doi.org/10.26896/1028-6861-2018-84-1(II)-49-53

Abstract

Potentialities of the method of inductively coupled plasma-atomic emission spectrometry (ICP- AES) in determination of the low content (0.001 – 0.01%) of aluminum in steels are studied. Analytical lines of aluminum and optimum operating parameters of Al determination are specified along with the choice of the sample preparation procedure. A technique for determination of the mass fraction of aluminum in the standard samples of carbon and low alloyed steels is developed. Indicators of the accuracy of the obtained results match the requirements specified for the accuracy of Al determination in the products of ferrous metallurgy.

About the Authors

G. N. Popkova
Institute for Certified Reference Materials
Russian Federation

Galina N. Popkova.

Yekaterinburg


V. V. Bazyanova
Institute for Certified Reference Materials
Russian Federation

Veronika V. Bazyanova.

Yekaterinburg


Yu. N. Shakhova
Institute for Certified Reference Materials
Russian Federation

Yuliya N. Shakhova.

Yekaterinburg


References

1. RF State Standart GOST R 51685–2013. Rails. General specifications. — Moscow: Standartinform, 2014. — 102 p. [in Russian].

2. Vinogradov A. P. Analytical chemistry of aluminium. — Moscow: Nauka, 1971. — 266 p. [in Russian].

3. Tikhonov V. N., Yakovlev P. Ya. Determination of aluminium in metals and alloys. — Moscow: Metallurgiya, 1978. — 264 p. [in Russian].

4. Kharlamov I. P., Eremina G. V. Atomic absorbtion analysis in ferrous metallurgy. — Moscow: Metallurgiya, 1982. — 166 p. [in Russian].

5. RF State Standart GOST 22536.10–88. Carbo steel and unalloyed cast iron. Metghod of aluminium determination. — Moscow: Izd. Standartov, 2001. — 11 p. [in Russian].

6. ASTM E350-12. Standard Test Methods for Chemical Analysis of Carbon Steel, Low-Alloy Steel, Silicon Electrical Steel, Ingot Iron, and Wrought Iron. — USA, 2012. — 65 p.

7. Pupyshev A. A., Danilova D. A. The use of inductively coupled plasma atomic emission spectrometry for analysis of materials and products of ferrous metallurgy / Analit. Kontrol. 2007. Vol. 11. Т 2 – 3. P. 131 – 181 [in Russian].

8. RF State Standart GOST R 55079–2012. Steel. Method of inductively coupled plasma atomic emission analysis. — Moscow: Standartinform, 2016. — 29 p. [in Russian].

9. Zaidel’ A. N., Prokof’ev E. K., Raisky S. M., Shreider E. Ya. Tables of spectral lines. — Moscow: Fizmatgiz, 1962. — 608 p. [in Russian].

10. STO 20872050. SMK. SK.09–2013. Mathematical and statistical processing of the results of determination of chemical composition of reference materials.. — Yekaterinburg: ZAO «ISO», 2013 [in Russian].


Review

For citations:


Popkova G.N., Bazyanova V.V., Shakhova Yu.N. DETERMINATION OF ALUMINUM IN STEEL BY INDUCTIVELY COUPLED PLASMA-ATOMIC EMISSION SPECTROMETRY (ICP-AES). Industrial laboratory. Diagnostics of materials. 2018;84(1(II)):49-53. (In Russ.) https://doi.org/10.26896/1028-6861-2018-84-1(II)-49-53

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ISSN 1028-6861 (Print)
ISSN 2588-0187 (Online)