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Long-term stability of measurements of the elemental composition of steel using a vacuum atomic emission spectrometer «Grand-Expert»

https://doi.org/10.26896/1028-6861-2019-85-1-II-135-138

Abstract

A study of the repeatability and long-term stability of elemental content measurements in a UG20 standard sample using a vacuum atomic emission spectrometer «Grand-Expert» was carried out on time scales of 10 min and 1 h. The values of standard and expanded uncertainty of the results of carbon, chromium, manganese, nickel and silicon determination which characterize the repeatability and long-term stability of measurements were calculated. It has been shown that a vacuum atomic emission spectrometer «Grand-Expert» provides determination of the content of alloying elements in steel with a relative expanded uncertainty of 1 – 2% whereas measurements of carbon content are characterized by higher relative expanded uncertainty of about 3%.

About the Author

I. N. Kuropyatnik
Technological Design Institute of Scientific Instrument Engineering of the Russian Academy of Sciences
Russian Federation
Novosibirsk


References

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Review

For citations:


Kuropyatnik I.N. Long-term stability of measurements of the elemental composition of steel using a vacuum atomic emission spectrometer «Grand-Expert». Industrial laboratory. Diagnostics of materials. 2019;85(1(II)):135-138. (In Russ.) https://doi.org/10.26896/1028-6861-2019-85-1-II-135-138

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ISSN 1028-6861 (Print)
ISSN 2588-0187 (Online)